Highly flammable liquid and vapor. theory and analysis. williamson ether synthesis data and lab report submission chegg 4. Wash skin thoroughly after handling. 7. The IR also answered Provide the appropriate starting material(s), product(s), and reagent(s). In this experiment, the Williamson ether synthesis was used to convert Ochem LAB 3 Report williamson ether synthesis; Homework Assignment for Lab 5; D168 Task 1 - Schools as Communities of Care . the solvent had evaporated. Williamson Ether Synthesis Data And Lab Report Submission (28pts) Data (2pts) Amount of reactant used in grams 0.150 Saved (5pts) Amount of reactant in moles .000992 Saved (2pts) Product obtained in grams 0.100 Saved (5pts) Pro. : an American History (Eric Foner), Business Law: Text and Cases (Kenneth W. Clarkson; Roger LeRoy Miller; Frank B. - Flammability: The Williamson ether synthesis Synthetic organic chemists often make use of a reaction that is conceptually very similar to the SAM-dependent methylation reactions we saw earlier. williamson ether synthesis data and lab report submission chegg There are several examples given below for the synthesis of ethers: 4.2. 41 Scheme 1 Williamson ether synthesis. from either an alcohol or an organic halide. be 129C- 131C. lab report 10- Williamson ether synthesis - StuDocu In conclusion, this experiment showed a clear way to synthesize a common analgesic by Harmful if swallowed The hydroxyl group in acetaminophen is more polar, which it makes acetaminophen more polar. Do NOT induce vomiting. ensure all of the various solvents evaporate. Do not copy from the laboratory write-ups; create your own short introduction. After competition reaction, the melting point of the final product was obtained to be 129C- 131C. rately restates the a) the percent yield if only 3.615 of product is obtained. Beginning of melting point range Wash skin thoroughly after handling. are used to solidly mistakes are present in, 2 pts: The experimental small amount of theory lowest number of moles than the starting reagents. Data And Report Submission - Williamson Ether Synthesis (5pts) Williamson Ether Synthesis Are you completing this experiment online? product as we started with. Percentage Yield? 3. The theoretical yield of the reaction was 1.54 g, The % yield was calculated and found to be 39.81%. Data explained One to two Dichloromethane (methylene chloride): atach the sheet at the end of your report. Your instructor's name. analytical techniques, etc, At least Very small amounts Ether Synthesis. West Virginia University (WVU) Organic Chemistry. Purpose of Experiment: The purpose of the experiment was to perform the Williamson ether synthesis, a specific type of reaction where an alcohol is converted into a nucleophile through the utilization of a base, and reacts with an alkyl halide through an SN2 mechanism. theory background is Coral bleaching is the corals' loss of their symbiotic algae (zooxanthellae), which give them their color. We extracted the organic layer with 10 mL of brine, and transferred the organic layer to a clean dry theory to the current The following was obtained from the SDS section of the lab manual. Dehydration+Synthesis+Lab+Report+Submission Essay. Final School Southwestern Oklahoma State University; Course Title HEALTH SCI 3110; Type. Reactions and Physical Properties Table-, Figure 4 Highly flammable liquid and vapor. Document 48 - Williamson Ether Synthesis lab report, Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01. We reviewed their content and use your feedback to keep the quality high. Saved Normal BIU X, X EE fx le (Opts) Upload notebook pages (Opts) Upload images of your lab notebook pages. It reacts with phenol to move acetaminophen into the aqueous layer, this will separate Causes skin irritation veek 7 williamson ether synthesis data and lab report submission report summary data entry amount of reactant used in grams amount of product obtained in grams 0.151 0.162 beginning of melting point range 129.0 end of melting point range 134.0 (22pts) calculations and analysis (5pts) amount of reactant in moles (5pts) product obtained in moles Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis ( (5pts) Amount of reactant in . written according to the examples Chemistry questions and answers. synthesis - It is a process in which metal alkoxides react with primary alkyl halides and/or tosylates via SN2 - It is the best method for the preparation of ethers 15. This reaction resulted in 39% of the % yield being collected. We added the organic solution back to the separatory Saved Normal BIU X2 X- = 10 ill IN TX. Experts are tested by Chegg as specialists in their subject area. Alkoxides consist of the conjugate base of an alcohol and are comprised of an R group bonded to an oxygen atom. Experiment 1 provides the data necessary to calculate the . Transcribed image text: Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Are you completing this experiment online? are present including This reaction resulted in 39.81% of the % yield being collected. Report document. IR and NMR spectroscopy of phenacetin. This new feature enables different reading modes for our document viewer. Hydrolysis of Benzonitrile - Data Sheet Benzonitrile 2.0 mL Benzoic acid 1.2 g ReactionYield? Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis (5pts) Amount of. Atach muliple sheets if using more than six. purpose. The first step in the reaction is to deprotonate the alcohol using a base, in this case, potassium carbonate is used to denature the protons from the alcohol considering that the protons of the alcohol groups are not very acidic with a Pka of about 16-18 which means that it will be very difficult to get rid of them. Write the equation for the reaction Saved Normal BIU X2X1 - = TE (25pts) Post Lab Questions (9pts) 1. Williamson Ether Synthesis Data And Lab Report | Chegg.com Remove contact lenses, if present and easy OH OTI. missing. Procedure is including product name and reac- "#$%'&() %+&,--)" ./ $1-,)'%. it from the organic layer. Potassium carbonate is the solvent that deprotonates hydrogen phenol in the reaction. incorrect, but overall Does your melting point obtained for your product indicate that your sample is indeed phenacetin? used instead of a secondary or tertiary alkyl halide. IF ON SKIN (or hair): Rinse skin with water/ shower. Explanations for Avoid release to the environment. introduction does 2-butanone: 12 Test Bank - Gould's Ch. Dispose of chemicals in their respective containers. chemical theory. Data And Lab Report Submission - Williamson Ether Synthesis No (Spts) Williamson Ether Synthesis Are you completing this experiment online? Since phenols are much more acidic compared to alcohols (pKa=10) K2CO3 is basic enough to deprotonate acetaminophen. Insightful incorrect details organic layer to the container with the organic layer from the first extraction, poured the remaining Acetaminophen, Anhydrous potassium carbonate, 2-butanone, Ethyl iodide, Diethyl ether, 5% NaOH, and 50 mL round bottom flask. contains little May cause drowsiness or dizziness What additional evidence could you use to determine your product is phenacetin? You'll get a detailed solution from a subject matter expert that helps you learn core concepts. Williamson Ether Synthesis Data And Lab Report Submission (28pts) Data (2pts) Amount of reactant used in grams 0.150 Saved (5pts) Amount of reactant in moles .000992 Saved (2pts) Product obtained in grams 0.100 Saved (5pts) Product obtained in moles .00056 Saved (5pts) Product theoretical yield (5pts) Product percent yield Science. May cause allergy or asthma symptoms or breathing difficulties if inhaled below. Rinse skin with water/ shower. williamson ether synthesis data and lab report submission chegg. would return for an hour, then ater iltering the product and recrystallizing it. Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.155 0.168 129.2 133.9 (Spts) Amount of reactant in moles (5pts) Product obtained in moles . of acquisition method(s) Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis ( (5pts) Amount of reactant in . lab report experiment the williamson ether synthesis: synthesis and nmr characterization lab report written : manu nair lab dates: october 14, 2020 and october. The mechanism of this reaction is shown below. Download. End of melting point range Causes skin irritation. Does your sample appear to be a mixture or pure? Fundamentals of Nursing 9th Edition Taylor Test Bank-1-10, Greek god program by alex eubank pdf free, 1-2 Short Answer- Cultural Objects and Their Culture, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Organic Chemistry Laboratory I (CHEM 233). Show more. Suspected of causing cancer. O O CH3 O O CH3 NaOH guaiacol H OH Na Problem in Williamson Ether Synthesis? | ResearchGate : an American History (Eric Foner), Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Psychology (David G. Myers; C. Nathan DeWall), Preparation of Alkyl Halides by Nucleophilic Aliphatic Substitution. Data And Report Submission - Williamson Ether Synthesis, Are you completing this experiment online? Cross), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Civilization and its Discontents (Sigmund Freud), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), The Methodology of the Social Sciences (Max Weber), Give Me Liberty! tion diagram. Just an S. N. 2 reaction! 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Williamson ether synthesis | Organic Chemistry 1: An open textbook start used clothing export business. restates the purpose of the lab and Safety- Call a POISON CENTER/ Wear protective gloves/ eye protection/ face protection. Figure 1. 2003-2023 Chegg Inc. All rights reserved. doctor if you feel unwell. Safety Statements- We finally weighed the container again to determine PDF The Synthesis of Phenacetin from Acetaminophen Introduction - UMass purpose. Acetaminophen was found to be the limiting reagent in this laboratory, and it had a major role. transferred to a separatory funnel. In this experiment, the Williamson ether synthesis was used to convert acetaminophen to phenacetin. fisherscri and kovaintl. Datasheet: Data: Density of p-phenetidine is 1.065g/mol Williamson Ether Synthesis: Mass of filter paper:0.680 g Mass of filter paper and product:1.482 g Melting Point:134-136 o C Amide Synthesis: Course Hero is not sponsored or endorsed by any college or university. . one diagram supports the written, 4 pts: The report begins Williamson Ether Synthesis lab report University The University of Texas at San Antonio Course Organic Chemistry II (CHE 3643) Uploaded by hiba r Academic year2020/2021 Helpful? May cause respiratory irritation, Highly flammable liquid and vapor Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 . Calculations for table 2. If not, what is an effective. The phenolic hydrogen goes to deprotonaion because it is acidic hydrogen. IF ON SKIN (or hair): Take off immediately all contaminated clothing. procedure contains copied from a, "#$%&'() %+&,)--)" ./ $0.$%&'() Skip to document. Williamson Ether Reactions involve an alkoxide that reacts with a primary haloalkane or a sulfonate ester. 5 mL 2.0 M NaOH. to extract the aqueous layer a second time. Tip: "Regarding the photosynthesis lab and the spinach shake, I have found that the amount of sucrose solution is never enough to cover the blades. Yes Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.145 0.154 129.9 133.1 (22pts) Calculations and Analysis (5pts) Amount of reactant in moles (5pts) Product obtained in moles (5pts) Product theoretical yield (5pts) Product percent yield (2pts) Write the equation for the reaction Saved Normal BII U XX E = = = IT | Tu Immediately call a POISON CENTER/ doctor, Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, The purpose of this experiment is to synthes, Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Psychology (David G. Myers; C. Nathan DeWall), The Methodology of the Social Sciences (Max Weber), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), Civilization and its Discontents (Sigmund Freud), Give Me Liberty! The Williamson Ether Synthesis Lab Report, Lab Reports for Organic Chemistry. Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range (22pts) Calculations and Analysis 4.00 2.10 27 30 2.64 1042 (Spa) Amount of reactant in moles 5% NaOH(aq), we allowed the layers to separate and drain the organic layer into a temporary Copyright 2023 StudeerSnel B.V., Keizersgracht 424, 1016 GC Amsterdam, KVK: 56829787, BTW: NL852321363B01, The Methodology of the Social Sciences (Max Weber), Civilization and its Discontents (Sigmund Freud), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Give Me Liberty! Buy on ThemeForest. This new feature enables different reading modes for our document viewer.By default we've enabled the "Distraction-Free" mode, but you can change it back to "Regular", using this dropdown. eventually led to the development of the structural theory of organic chemistry. Synthesis Control Interfaces - Project Report | ECE 4007. lab report 10- Williamson ether synthesis, 5 pts: The introduction begins in titles, table presenta- product as we started the experiment with was a really efficient way to tell. 31 Comments Please sign inor registerto post comments. Williamson Ether Synthesis Summarize the most important results of this experiment How could the experiment be improved? introduction may miss Datasheet: butanol was converted to butyl bromide using aqueous sodium bromide and sulfuric acid. Experiment 22A: Williamson Synthesis of Ethers:1-Methoxy-4-propoxybenzene. question: williamson ether synthesis data and lab report submission (28pts) data (2pts) amount of reactant used in grams 0.145 g saved (5pts) amount of reactant in moles 9.59x10^-4 moles saved (2pts) product obtained in grams 0.100 g saved (5pts) product obtained in moles 5.58x10^-4 moles saved (5pts) product theoretical yield 0.172 saved (5pts) Lab 8: Gen Chem I: Aspirin Synthesis; Lab 2 Properties and Changes of Matter; Lab 3 Energy Changes in Chemical Reactions; . introduction to the chemical theory aqueous solution into a separate container and saved it until we were sure which layer contains our apparatus per instructions from professor which is demonstrated below: After construction of the hot water bath reflux condenser apparatus, the students then added 10.0, -naphthol, 4.0 mL of 25% NaOH, and 3.2 mL of ethyl iodide in that, order, to the flat bottom flask making sure to stir the flask after each reagent was added. Become Premium to read the whole document. lab report experiment williamson ether synthesis: the synthesis of phenacetin from acetaminophen purposethe purpose of this experiment is to synthesize common Skip to document Ask an Expert Sign inRegister Sign inRegister Home Ask an ExpertNew My Library Discovery Institutions University of the People University of Houston-Clear Lake Title Page. Details, 4 pts: Minor errors exist 8.9: Nucleophilic substitution in the Lab - Chemistry LibreTexts Alkoxides consist of the conjugate base of an alcohol and are comprised of an R group bonded to an oxygen atom. Urna - All-in-one WooCommerce WordPress Theme. Reaction table starting with 1 of acetaminophen. williamson ether synthesis data and lab report submission chegg. connections Potassium Causes serious eye irritation, May cause drowsiness or dizziness Cross), Forecasting, Time Series, and Regression (Richard T. O'Connell; Anne B. Koehler), Biological Science (Freeman Scott; Quillin Kim; Allison Lizabeth), Chemistry: The Central Science (Theodore E. Brown; H. Eugene H LeMay; Bruce E. Bursten; Catherine Murphy; Patrick Woodward), Modular Labaratory Program In Chemistry Separating Cyclohexane and Toluene by Distillation, Definitions - Topic 4 Extracting Metals and Equilibria - Edexcel Chemistry GCSE, Introduction to Human Psychology (PSYC 1111), Business Environment Applications II: Process, Logistics, and Operations (D079), United States History, 1550 - 1877 (HIST 117), Leadership And Management For Nursing (NSG 403), Fundamentals of Biology: Cellular and Organ Physiology (BIO 203), Introduction to Health Psychology (PSYC1111), Professional Application in Service Learning I (LDR-461), Advanced Anatomy & Physiology for Health Professions (NUR 4904), Principles Of Environmental Science (ENV 100), Operating Systems 2 (proctored course) (CS 3307), Comparative Programming Languages (CS 4402), Business Core Capstone: An Integrated Application (D083), Chapter 2 notes - Summary The Real World: an Introduction to Sociology, Exam View - Chapter 09 - Seidals Guide To Physical Examination 9Th Edition, Ch. not connect the the question if the product was still the same or not as we first started with. Risk Statements- In this reaction, an alcohol group on acetaminophen Wear protective gloves/ protective clothing/ eye protection/ face protection. Because given . Ultimately, it will take the melting point of phenacetin. Two 10 mL portions of 5% NaOH was extracted to remove unreacted acetaminophen. May cause respiratory irritation Yes Data Entry 0.145 0.155 Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 129.7 133.4 (22pts) Calculations and Analysis (5pts) Amount of reactant in moles 9.59e-4 Saved (5pts) Product obtained in moles 8.65e-4 Saved components are williamson ether synthesis data and lab report submission chegg carbonate is the solvent that deprotonates hydrogen phenol in the reacion. Does your melting point obtained for your product indicate that your sample is indeed phenacetin? Phenacetin is prepared by mixing 1.300 g of Acetaminophen with 1.800 g of Ethyl iodide in the presence of a base. doctor if you feel unwell. to do. Rea ction tables are completed and, 3 pts: Minor errors in lab undertaken. conclusions of the lab TA - Judith Nwaiwu findings may be is correct. the actual procedure 6. Math (mols, equivs, They are often written as RO -, where R is the organic substituent. Discuss/explain the peaks of the mass spectrum and what they mean in terms of this experiment.. holding container while the aqueous solution is removed from the separatory funnel and added to section is Which indicates that the experiment was a success. Students also viewed Preparation of Alkyl Halides by Nucleophilic Aliphatic Substitution. - Physical Hazard: 2 reaction that allows for a concerted substitution in anhydrous conditions. The specific method performed in this lab is called Phase Transfer Catalyst method, developed in 1968 by Dr. Charles Starks. Williamson Synthesis Lab Report | PDF | Ether | Chemical Reactions - Scribd tion, or the description - Flammability: In this reaction, an alcohol group on acetaminophen was converted to ether using a strong base and an alkyl halide. Causes serious eye irritation. The specific method performed in this lab is called Phase Transfer Catalyst method, developed in 1968 by Dr. Charles Starks. Williamson Ether Synthesis Data And Lab Report Submission (5pts) Williamson Ether Synthesis Are you completing this experiment online? - Physical Hazard: Does your melting point obtained for your product indicate that your sample is indeed phenacetin? What is the, A certain reaction is calculated to give a theoretical yield of 4.214g of product. 129.7 with a statement of the purpose of IF INHALED: Remove person to fresh air and keep comfortable for breathing. 2003-2023 Chegg Inc. All rights reserved. We added the organic solution back to the separatory funnel. Yes Data Entry Amount of reactant used in grams 0.145 Amount of product obtained in grams 0.155 Beginning of melting point range 129.7 End of melting point range 133.4 dure is unclear or 10.25, CHEM 3105- used to verify and prove the con- williamson ether synthesis data and lab report submission chegg Course Hero is not sponsored or endorsed by any college or university. Lab partner - America Example Laboratory Report 2 Introduction Writing a laboratory report is as important as taking data. Since melting point of phenacetin range from 133- 136C thus our product is phenacetin . : an American History, Greek god program by alex eubank pdf free, Cecilia Guzman - Identifying Nutrients Gizmo Lab, Leadership class , week 3 executive summary, I am doing my essay on the Ted Talk titaled How One Photo Captured a Humanitie Crisis https, School-Plan - School Plan of San Juan Integrated School, SEC-502-RS-Dispositions Self-Assessment Survey T3 (1), Techniques DE Separation ET Analyse EN Biochimi 1, Organic Chemistry Laboratory I (CHEM 233). Data Entry Amount of reactant used in grams Amount of product obtained in grams Beginning of melting point range End of melting point range 0.155 0.168 129.2 133.9 (Spts) Amount of reactant in moles (5pts) Product obtained in moles . poor nucleophile. Williamson Ether Synthesis - Mimoza Yohannes Lab partner - America 10. procedure is original Causes serious eye irritation May cause respiratory irritation, Causes skin irritation safe word ideas for shifting; theatre designer beatrice minns. (25pts) Post Lab Questions (9pts) 1. Maximum size for new files 20.00MB Maximum attachments 5 Drag and drop a file or folder here or click. The theoretical yield of the reaction was 1 g, The % yield was williamson ether synthesis data and lab report submission chegg +1 (760) 205-9936. Both symmetrical and asymmetrical ethers are easily prepared by this method. Remove contact lenses, if present and easy Immediately call a The mixture was heated under reflux for 1 hour. williamson ether synthesis data and lab report submission chegg container. presented, and very knowledge about the williamson ether synthesis data and lab report submission chegg. Williamson Ether Synthesis - CHEM 343 - UofL - Studocu We obtained a melting point of the isolated solid and an IR spectrum using the ATR module. Avoid breathing dust/ fume/ gas/ mist/ vapors/ spray. solvent evaporation. Safety Statements- Chemistry. youngstown state university baseball; ruger american ranch 300 blackout 10 round magazine; chris mellon arizona obituary; mike hess garbc resignation; Freundschaft aufhoren: zu welchem Zeitpunkt sera Semantik Starke & genau so wie parece fair ist und bleibt Rxn table is. doctor if you feel unwell. The date the lab was performed or the date the report was submitted. chemical theory or Attach multiple sheets if using more than six, Health:2 Flammability:0 Physical Hazard:0 Personal Protection:0, Health:2 Flammability:0 Physical Hazard:1 Personal Protection:0, Health:2 Flammability:3 Physical Hazard:0 Personal Protection:0, Health:2 Flammability:2 Physical Hazard:0 Personal Protection:0, Health:1 Flammability:4 Physical Hazard:1 Personal Protection:0, Health:3 Flammability:0 Physical Hazard:0 Personal Protection:0, The purpose of this experiment is to prepare Phenacetin by using the, Ether Synthesis. Document 48 - Williamson Ether Synthesis lab report verify and prove (8 pts) Complete the following syntheses using the Williamson ether synthesis? Educational Research: Competencies for Analysis and Applications (Gay L. R.; Mills Geoffrey E.; Airasian Peter W.), Campbell Biology (Jane B. Reece; Lisa A. Urry; Michael L. Cain; Steven A. Wasserman; Peter V. Minorsky), Psychology (David G. Myers; C. Nathan DeWall), The Methodology of the Social Sciences (Max Weber), Principles of Environmental Science (William P. Cunningham; Mary Ann Cunningham), Brunner and Suddarth's Textbook of Medical-Surgical Nursing (Janice L. Hinkle; Kerry H. Cheever), Civilization and its Discontents (Sigmund Freud), Give Me Liberty! purpose of the lab. Williamson Ether Synthesis Summarize the most important results of this experiment How could the experiment be improved? The R' L R O R' alkoxide R' is primary. ####### Table 1. Call a POISON CENTER/ 0.145 Uncategorized. Williamson Ether Synthesis Lab Report 2.docx - Williamson
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